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The Chemical Educator

ISSN: 1430-4171 (electronic version)

Table of Contents Vol. 19 Pages 1-all

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Extraction and Quantification of Insecticides From Bananas Using a QuEChERS-GC-NPD Method
Lidia María Ravelo-Pérez—1
Article in PDF format (177 KB) HTML format

Free Radical Generation and Inhibition With Luminol and Ascorbic Acid (AA)
Charles F. Saladino*, and Adaline Predmore—6
Article in PDF format (182 KB) HTML format

Utilizing Smart Devices as Eductional Tools to Study First Order Substitution Reactions of tert-butyl Halides in the Classroom Setting
Emily R. Vogel, Maureen E. Smith, Douglas S. Masterson*—11
Article in PDF format (41 KB) HTML format

Combining FTIR Spectroscopy and the Vernier Gas Chromatograph: Analysis of a Binary Mixture
Logan A. Schmitz, Kimberly A. Gerling, Joseph M. Fritsch, David B. Green*—14
Article in PDF format (62 KB) HTML format

Kinetic Study of Catalytic Decomposition of Hydrogen Peroxide by Aqueous Fe3+ Ion ― A Green Chemistry Approach
Mala Das Sharma* and M. Karuna—18
Article in PDF format (137 KB) HTML format

Stimulating the Imagination: A Green Tech, Deep Ocean Retrieval System
Cody Moncrief, Eric Haas, Elizabeth A Atkinson, Donna F Law, Brett Little, Chelsie D Northcutt, Ryndell Langford, Hilary F Lee, Gregory A Jackson, Jenna L Lippincott, Nicholas Fight, and Thomas Manning*—22
Article in PDF format (341 KB) HTML format

Less Cookbook and More Research! Synthetic Efforts Toward JBIR-94 and JBIR-125: a Student-Designed Research Project in a Sophomore Organic Chemistry Lab
Michael A. Christiansen,* Cathy L. Crawford, Chad D. Mangum—28
Article in PDF format (111 KB) HTML format

An Adiabatic Expansion Experiment Done On A Budget
Jason Hofstein*, Michael Perry, and Daniel McCabe—34
Article in PDF format (67 KB) HTML format

Simple Colligative Properties Laboratory Experiment
David K. Dalby—39
Article in PDF format (377 KB) HTML format

An Experiment Utilizing Corrosion of Aluminum to Illustrate a Contracting Volume Rate Law
Thomas B. Sobyra and James E. House*—45
Article in PDF format (233 KB) HTML format

US-Africa Collaboration in a Chemical Education Project Involving Analysis of AmaranthusGrain Oil from Selected Agro-Ecological Zones in Kenya
Joseph K. Rugutt*, Kevin Otieno Okoth, Ruth N. Wanjau, Nicholas K. Gikonyo, Alex Machocho, Kipgeno J. Rugutt, KristinaY. Rykhlya, Keil B. Harris, Katie R. Wilson, and Joel Koech—50
Article in PDF format (47 KB) HTML format

Synthesis and Analysis of Aspirin in Three Hours: Protocol Optimization and TLC/HPLC Analyses Result in Improved High School/Non-Science Major Student Success
Christa A. Currie—55
Article in PDF format (335 KB) HTML format

Square Wave Anodic Stripping Voltammetry Analysis of Arsenic Using Solid Gold and Silver Electrode
Corrie Spradlin, Phuong Khanh Quoc Nguyen and Suzanne Lunsford*—58
Article in PDF format (195 KB) HTML format

Microwave Assisted Depolymerization of Post Consumer PET Waste Using Phase Transfer Catalysts
T. Jaba Priya, Subramee Sarkar , G. Shamili and R.Wilfred Sugumar*—61
Article in PDF format (175 KB) HTML format

Integrating Chemical Information Skills in a Problem-Based Second Semester Organic Chemistry Laboratory toward the Synthesis of Adipic Acid
Ryan E. Denton* and Eric A. Snajdr—64
Article in PDF format (230 KB) HTML format

Presumptive and Confirmatory Tests using Analogs of Illicit Drugs: An Undergraduate Instrumental Methods Exercise
Benjamin D. Rouse, Rebecca L. Schneider, and Eugene T. Smith*—70
Article in PDF format (102 KB) HTML format

Nobel Prize for MRI Imaging Denied to Raymond V. Damadian a Decade Ago
George Kauffman*—73
Article in PDF format (1.9 MB) HTML format

A Quantitative Analytical Chemistry Research-based Experiment Involving Comparative Analysis of Amaranth Grain Oils Extracted from Embu and Meru Districts in Kenya
Joseph K. Rugutt*, Kevin Otieno Okoth, Ruth N. Wanjau, Nicholas K. Gikonyo, Alex Machocho, Kipgeno J. Rugutt, Millie Chepkemoi Obel, and Erick Mibei—91
Article in PDF format (32 KB) HTML format

An Automated Titrator Based on a Microcontroller: an Interfacing Exercise for Advanced Analytical Chemistry Students
Gary A. Mabbott—96
Article in PDF format (622 KB) HTML format

Chemistry and the International Year of Light
Sameen Ahmed Khan—102
Article in PDF format (37 KB) HTML format

A Sublimation Experiment with Unknowns
Kate J. Graham*, Abdimahad S. Nur and Chris P. Schaller—104
Article in PDF format (39 KB) HTML format

Karl Karlovich Klaus (1796–1864) and the Discovery of Ruthenium
George B. Kauffman,*James L. Marshall, and Virginia R. Marshall—106
Article in PDF format (426 KB) HTML format

Frederick Sanger (1918–2013), Founder of Genomics and the Only Two-Time Nobel Chemistry Laureate: An Obituary-Tribute
George B. Kauffman*and Jean-Pierre Adloff—116
Article in PDF format (703 KB) HTML format

Buret Experiment to Explore Correlations between Physical and Chemical Properties of Alcohols and Salt Solutions
Rachel T Mikula, Aaron T Calvin, Willis W Brown, Stephen I Edwards, Bianca S Farley, Haley A Franklin, Rebekah E Graham, Jermila S Ingram, TysheonMcGreggor, Andrew J Mock, Alesia Nicole Neloms, Chelsie D Northcutt, Mehulkumar P Patel, Rachel L Robertson, Frankie A Stackhouse, Gregory R Anzalone, Pamela L Brown, Andrew V DeLong, Anthony J Fino, Alexis B Garza, Ashley G Humphries, Brittany S Larcart, James C Lord, Chandler B Massey, Tyler L Peterson, Michael J Reaves, Jeffrey M Roland, Keyanna M Seville, Thomas Manning*, Aurora Pérez Gramatges—125
Article in PDF format (2.16 MB) HTML format

Greening the Inorganic Lab: Combining Microwaves and Phase Transfer Catalysis for the Rapid Synthesis of Group VI Carbonyl Complexes
Kurt R. Birdwhistell*, Kathryn J. Conroy, and Brian E. Schulz—133
Article in PDF format (131 KB) HTML format

Student-Centered, Guided Inquiry Physical Science: A Novel Approach to Modeling Authentic Science for Pre-Service Teachers
Jeff S. Piquette*—138
Article in PDF format (42 KB) HTML format

Signal to Noise Ratios Verses Cold Fusion Student Led Experiment with High Voltage, High Frequency Discharge
Aaron Calvin, Thomas Manning*, Russ Goddard, JimHappell—144
Article in PDF format (504 KB) HTML format

An Automatic Grading System For a Laboratory Experiment Class: Kinetic Determination of Furfural as a Parameter of Food Quality
María Isabel Rodríguez-Cáceres†,Nielene Mora-Diez†,María P. Godoy-Caballero†, David Muñoz de la Peña‡, David González Gómez§ and Arsenio Muñoz de la Peña*,†—148
Article in PDF format (174 KB) HTML format

An Alternative Approach to Titrating Fe2+(aq) in Dietary Supplement Tablets Using Electrolytically Produced Ce4+(aq)
Huirui Washington, Christopher Scanlon, Samuel Melaku, James O. Schreck, and Rajeev B. Dabke*—153
Article in PDF format (223 KB) HTML format

Microwave Synthesis of Chromium(III) Complexes with Acetylacetonate and Ethylenediamine Ligands
Joel A. Dopke*, Nancy Carter Dopke*, and Jared Kilpatrick—157
Article in PDF format (124 KB) HTML format

The Effect of a Few Key Parameters on the Instrumental Analysis of Fatty Acid Methyl Esters (FAME) in Biodiesel by Gas Chromatography-Mass Spectrometry (GC-MS)
Wes E. Steiner* and Kelsey A. Morrison —160
Article in PDF format (539 KB) HTML format

Games, Games, Games; Playing to Engage with Chemistry Concepts
Michael J. Samide and Anne M. Wilson—167
Article in PDF format (35 KB) HTML format

Isolation, Characterization and Utilization of Horseradish Peroxidase:  A Multiweek Undergraduate Biochemistry Laboratory
Kathryn Mansfield Matera—171
Article in PDF format (412 KB) HTML format

A Breadboard Filter Photometer/Fluorometer that Illustrates the Effects of Spectral Bandpass on Calibration Curves While Measuring Free-Chlorine in Tap Water and Quinine in Tonic Water
Tyler Tommey, Dustin Wagner, John Shaw Jr., and Michael K. Bellamy*—175
Article in PDF format (234 KB) HTML format

Use of WolframAlpha in Equilibrium Calculations
David A. Cleary—182
Article in PDF format (184 KB) HTML format

An Inquiry Study into the Acylation Reaction Requirements for the Organic Chemistry Laboratory: Customizing the Synthesis of Aspirin
Fernanda M. Burke* and Drashti Patel—187
Article in PDF format (542 KB) HTML format

The Crisis of Water Contamination Containing Lead and Detection of Heavy Metals by Square Wave Anodic Stripping Voltammetry
Corrie Spradlin, Mary Sullivan, Phuong Khanh Quoc Nguyen, and Suzanne Lunsford*—194
Article in PDF format (220 KB) HTML format

Using Microprocessor Based Laboratories to Enhance Chemistry Lectures
David P. Schuster—198
Article in PDF format (235 KB) HTML format

Nuclear Chemistry Under Western New York: A Lesson for General Chemistry
Dominic L. Ventura* and Angela D. Poblocki—205
Article in PDF format (711 KB) HTML format

Exploring Pioneer Women in Chemistry: Discoveries Amid Conflicts in a Study Abroad Course
Janis H. White, Valencia Browning Keen, and Rick C. White*—210
Article in PDF format (107 KB) HTML format

Some Examples of Redox Back Titrations
Tadeusz Michałowski* Agustin Garcia Asuero, Maja Ponikvar-Svet, Anna Maria Michałowska-Kaczmarczyk, Sławomir Wybraniec—217
Article in PDF format (209 KB) HTML format

Raman Spectroscopy of Allotropes of Carbon: An Undergraduate Laboratory
William Livernois, Christopher M. Crittenden, J. Brett Kimbrell, Farooq A. Khan, Anne C. Gaquere-Parker, and Douglas A. Stuart*—223
Article in PDF format (596 KB) HTML format

Teaching Quantum Numbers Using Candy: An Activity for a General Chemistry Course
Kelly M. Elkins—229
Article in PDF format (36 KB) HTML format

Are Slaters Rules the Best Approach for Calculating Effective Nuclear Charge for Undergraduates?
Preston Moore and Edward R. Birnbaum*—232
Article in PDF format (345 KB) HTML format

“Available Chlorine” In Household Bleaches by Using a New and Easy Spectrophotometric Method
Florencia Caucino, Ruth Calderón, Gimena Montes Spinsanti, and Andrés Ciolino*—236
Article in PDF format (221 KB) HTML format

Investigation of 1H NMR Chemical Shift in Various Systems: A Set of Advanced 1D 1H NMR Undergraduate Laboratory Projects
Laurie A. Witucki, William R. Winchester and Shannon M. Biros*—241
Article in PDF format (275 KB) HTML format

Fluorous Solvents for Slow Chlorination and Bromination of Alcohols
Elisabeth Rukmini Goei, Susan Sonchik Marine*, Richard T. Taylor, Angela French, Amanda E. Stewart*—247
Article in PDF format (242 KB) HTML format

Wilhelm Conrad Röntgen (1845–1923) at the University of Strasbourg: A Retrospective View for the 2014 International Year of Crystallography
Jean-Pierre Adloff and George B. Kauffman*—252
Article in PDF format (469 KB) HTML format

Living Polymerization
Ajay Kumar—257
Article in PDF format (97 KB) HTML format

An Introductory Physical Properties Laboratory Utilizing Materials Used in Jewelry-Making
Christine H. Jaworek-Lopes*, Naomi Lev, and Analice H. Sowell—261
Article in PDF format (48 KB) HTML format

Determination of Moisture Content of Over the Counter Pharmaceuticals and Dried Powdered Food Products Using Coulometric Karl Fischer Titration: A Summer Undergraduate Research Experience at Historically Black College and University
Sayo O. Fakayode*, Cameron Abel, David A. Pollard—264
Article in PDF format (95 KB) HTML format

Discussions of Chemistry in Jules Verne’s The Mysterious Island
James E. House*—269
Article in PDF format (48 KB) HTML format

Synthesis of Organic Semiconductor Backbone Using a Suzuki-Miyaura Cross-Coupling
Juha P. Heiskanen*—275
Article in PDF format (36 KB) HTML format

A Multivariable Enzymatic Resolution Laboratory Experiment
Edward J. McIntee*, Betsy J. Hutchinson and Kate J. Graham—276
Article in PDF format (384 KB) HTML format

Flame Atomic Absorption Spectroscopic Determination of Iron in Breakfast Cereals: A Validated Experiment for the Analytical Chemistry Laboratory
Ali Bazzi*, Judith Bazzi, Yiwei Deng, and Marwa Ayyash—283
Article in PDF format (266 KB) HTML format

A “One-Pot” Synthesis of Blattellaquinone
Brian E. Love* and Brian C. Duffy—287
Article in PDF format (37 KB) HTML format

Stephanie L. Kwolek, Inventor of Kevlar, Dies at 90
George B. Kauffman*—289
Article in PDF format (387 KB) HTML format

Undergraduate Research Experiences During January Academic Sessions
Neil L. Heckman* and Moses K. Dogbevias—296
Article in PDF format (25 KB) HTML format

Microwaving Metals: Inserting Metals into Porphyrin Ligands using Microwave Methods
Anne M. Arnold, Douglas J. Kwak, L. Elise Löfgren, Brittany M. Walters, Ashley L. Wilt, Selamawit A. Woldemeskel, and Edward P. Zovinka*—299
Article in PDF format (129 KB) HTML format

A 45MHz NMR Spectrometer as a Cost-Effective Option in Chemistry Teaching Labs
Suzanne Carpenter* and Richard Wallace—302
Article in PDF format (62 KB) HTML format

Lightning in a Bottle: Measuring NOx Formed by Electrical Discharge in an Inquiry-Based General Chemistry Laboratory Experiment
Kurt Winkelmann*, Monica H. Baloga, and Alfred Menendez—305
Article in PDF format (260 KB) HTML format

A Low-Cost Method for Measuring the Permeability of a Pharmaceutical Drug in a Diffusion Cell
Megan Kitson, Heather Sheppard, , Nicola M. Howarth*, and Arno Kraft*—310
Article in PDF format (223 KB) HTML format

Prediction and Modeling of Molecular Structure:An Exercise in Levels of Modeling for Students in General Chemistry
Michael W. Ducey* and David R. Myers*—314
Article in PDF format (62 KB) HTML format

Nobel Prizes During World War I (1914–1918), Part 1: Theodore W. Richard
George B. Kauffman*and Jean-Pierre Adloff—319
Article in PDF format (145 KB) HTML format

Hammett and Taft Equations are Tools for Identifying the Rate-Determining Step of a Multi-Step Reaction: A One Hour Class-Room Lecture to Graduate Students
Rachuru Sanjeev, Vandanapu Jagannadham*, Adam A Skelton and Rachuru Veda Vrath—327
Article in PDF format (120 KB) HTML format

Photolysis of a Cyclic Carbonate Ester and a Cyclic Sulfite Ester: Radical Intermediates and Ionic Intermediates in an Advanced Laboratory Experiment
Benny E. Arney, Jr.*, Jacob Perry, Nathan Thompson and Rick C. White*—330
Article in PDF format (133 KB) HTML format

Simultaneous Introduction of the Henderson-Hasselbalch Equation and Proton-Coupled Electron Transfer: An Undergraduate Laboratory Experiment
Anwesha Jana, Debarati Roy Chowdhury, Archana Singh*, and Amit Paul*—333
Article in PDF format (155 KB) HTML format

Analysis of Arsenic Concentration in Food Utilizing Graphite Furnace Atomic Absorption Spectroscopy
Wendy Lynn Burns—338
Article in PDF format (96 KB) HTML format

Biodiesel Synthesis, Viscosity, and Quality Control for an Introductory Chemistry Lab
Kenneth A. Walz*, Stephanie Britton, Jessica Crain, Katie Cadwell, Adam Hoffman and Paul Morschauser—342
Article in PDF format (25 KB) HTML format

A “Green” Approach to Synthesis of trans-4-Methoxycinnamic acid in the Undergraduate Teaching Laboratory
Kristopher J. Keuseman* and Nicole C. Morrow—347
Article in PDF format (97 KB) HTML format

Measuring Ibuprofen Quantities in Expired Over-the-Counter Tablets using HPLC and UV-VIS
Dan Y. Dong and Gordon G. Brown*—351
Article in PDF format (123 KB) HTML format

Polyeugenol Modified Electrode For Selective Determination of Neurotransmitter Catechol in the Presence of Ascorbic Acid on Different Working Electrodes
Corrie Spradlin, Mary Sullivan, Stamatina Tolias, and Suzanne Lunsford*—354
Article in PDF format (334 KB) HTML format

Investigation of the Mechanism of the Diet Soda Geyser Reaction
David E. Gardner, Bhargav R. Patel, Vicktoria K. Hernandez, Duncan Clark, Scott Sorensen, Kyle Lester, Yvette Solis, Dan Tapster, Adam Savage, Jamie Hyneman, and Albert D. Dukes, III*—358
Article in PDF format (90 KB) HTML format

Analysis of Nitroaromatic Explosives by High Performance Liquid Chromatography: A Laboratory Exercise for Quantitative Analysis
Darcey G. Wayment* and Glenn V. Lo—363
Article in PDF format (252 KB) HTML format

Guided Inquiry Learning to Teach Undergraduates Computational Aspects of Antibiotics
Andrew V DeLong; Jared C Harris; Brittany S Larcart; Chandler B Massey; Chelsie D Northcutt; Somuayiro N Nwokike; Oscar A Otieno; Harsh M Patel; Mehulkumar P Patel; Eugene I Rowell; Brandon M Rush; Marc-Edwin G Saint-Louis; Amy M Vardeman; Felicia N Woods; Pratik Pravin Patel; Giso Abadi, Thomas J. Manning*—367
Article in PDF format (20 KB) HTML format

Nobel Prizes During World War I (1914–1918), Part 2: Max von Laue (1879–1960)
George B. Kauffman*and Jean-Pierre Adloff—369
Article in PDF format (510 KB) HTML format

Reducing Heavy Metal Waste in Potentiometric Exercises in the General Chemistry Laboratory
Frazier Nyasulu*, Jenna Silverman, Brandon Allman, Rebecca Barlag, Phyllis Arthasery and Lauren McMills—379
Article in PDF format (194 KB) HTML format

Pressure-induced Ionization of Hydrogen: A Computational Project
Jonathan Hunt, James Martin, Vanessa Rosing, Josh Winner and Henry E. Montgomery, Jr.*—384
Article in PDF format (114 KB) HTML format

Nobel Prizes During World War I (1914–1918), Part 3: Richard Martin Willstätter (1872–1942)
George B. Kauffman*and Jean-Pierre Adloff—390
Article in PDF format (533 KB) HTML format


Online publication: 2014

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